1SZ0
N-terminal 3 domains of CI-MPR bound to mannose 6-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 103 |
Detector technology | IMAGE PLATE |
Collection date | 1999-06-10 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.100, 86.500, 84.800 |
Unit cell angles | 90.00, 109.57, 90.00 |
Refinement procedure
Resolution | 28.800 - 2.100 |
R-factor | 0.2381 |
Rwork | 0.238 |
R-free | 0.28700 |
Structure solution method | RIGID BODY REFINEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.800 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 45601 | |
Completeness [%] | 81.2 | 28.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.35 | 292 | 25% PEG 4000, 0.1M sodium cacodylate (pH 6.35), 150mM NaCl, 50 mM imidazole (pH 6.7), 10 mM manganese chloride, 5mM beta-glycerophosphate, 10 mM mannose 6-phosphate, VAPOR DIFFUSION, SITTING DROP, temperature 292K |