1SU6
Carbon monoxide dehydrogenase from Carboxydothermus hydrogenoformans: CO reduced state
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-01-01 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 112.154, 75.485, 71.260 |
| Unit cell angles | 90.00, 111.20, 90.00 |
Refinement procedure
| Resolution | 8.000 - 1.640 |
| R-factor | 0.157 |
| Rwork | 0.157 |
| R-free | 0.20170 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.000 |
| High resolution limit [Å] | 1.640 |
| Number of reflections | 66048 |
| Completeness [%] | 95.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 2-Propanol, PEG 3000, Hepes, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
