1SOX
SULFITE OXIDASE FROM CHICKEN LIVER
Experimental procedure
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-08-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.117, 197.690, 56.009 |
Unit cell angles | 90.00, 94.23, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.900 |
R-factor | 0.1748 |
Rwork | 0.175 |
R-free | 0.22020 * |
Structure solution method | MIR |
RMSD bond length | 0.009 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.8) |
Refinement software | X-PLOR (3.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.060 * | 0.160 * |
Number of reflections | 84147 | |
<I/σ(I)> | 11.4 | |
Completeness [%] | 89.2 | 66.2 |
Redundancy | 2.1 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.5 | 22 * | used to seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | reservoir | 0.65-0.9 (M) | ||
3 | 1 | reservoir | HEPES | 100 (mM) | pH7.5 |