1RZ1
Reduced flavin reductase PheA2 in complex with NAD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-02-20 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 53.693, 156.457, 83.925 |
| Unit cell angles | 90.00, 91.11, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.100 |
| R-factor | 0.23726 |
| Rwork | 0.237 |
| R-free | 0.25604 |
| Structure solution method | FOURIER SYNTHESIS |
| Starting model (for MR) | 1rz0 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.489 |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | CCP4 |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 15.000 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 77418 |
| Completeness [%] | 96.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
