1R9H
Structural Genomics of C.elegans: FKBP-type Peptidylprolyl Isomerase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-08-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 52.417, 52.417, 210.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 1.800 |
R-factor | 0.21 |
Rwork | 0.210 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 38.130 |
High resolution limit [Å] | 1.600 |
Number of reflections | 21526 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 1.6M ammonium sulfate, 0.1M MES, 10% dioxane, seeding was used to grow the crystals, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |