1QL7
FACTOR XA SPECIFIC INHIBITOR IN COMPLEX WITH BOVINE TRYPSIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1998-07-15 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.060, 58.580, 63.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.100 |
R-factor | 0.203 * |
Rwork | 0.200 |
Structure solution method | OTHER |
RMSD bond length | 0.008 |
RMSD bond angle | 24.600 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.111 | 0.425 |
Number of reflections | 13570 | |
<I/σ(I)> | 8.3 | |
Completeness [%] | 96.1 | 93.3 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 | 0.1M IMIDAZOLE PH8.0, 0.1M AMMONIUM SULPHATE, 20% PEG8K, pH 8.00 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | inhibitor | 2 (mg/ml) | |
3 | 1 | reservoir | imidazole | 0.1 (M) | pH8. |
4 | 1 | reservoir | ammonium sulfate | 0.1 (M) | |
5 | 1 | reservoir | PEG8000 | 20 (%) |