1PTX

CRYSTAL STRUCTURE OF TOXIN II FROM THE SCORPION ANDROCTONUS AUSTRALIS HECTOR REFINED AT 1.3 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	45.940, 40.680, 29.930
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 1.300
R-factor	0.148
Rwork	0.148
RMSD bond length	0.017
RMSD bond angle	0.028 *
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.300 *	1.300 *
Rmerge	0.120 *
Number of reflections	13619 *	597 *
Completeness [%]	94.6 *	86.1 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	seeding *	6.8 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	toxin	5-10 (mg/ml)
2	1	1		0.2 (M)