1PEN
ALPHA-CONOTOXIN PNI1
Experimental procedure
Temperature [K] | 289 |
Detector technology | IMAGE PLATE |
Collection date | 1995-09-28 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 15.000, 19.800, 16.500 |
Unit cell angles | 90.00, 113.40, 90.00 |
Refinement procedure
Resolution | 6.100 - 1.100 |
R-factor | 0.127 |
Rwork | 0.127 |
R-free | 0.15200 |
RMSD bond length | 0.005 |
RMSD bond angle | 22.700 * |
Data reduction software | DENZO |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 1.100 | 1.100 * |
Rmerge | 0.080 | 0.240 * |
Total number of observations | 16298 * | |
Number of reflections | 3459 | |
Completeness [%] | 94.0 | 80 * |
Redundancy | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 | 14 * | used to seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PnIA | 1.5 (mg/ml) | |
2 | 1 | drop | sodium potassium Tartrate | 0.1 (M) | |
3 | 1 | drop | Tris-HCl | 0.05 (M) | |
4 | 1 | reservoir | sodium potassium Tartrate | 0.2 (M) | |
5 | 1 | reservoir | Tris-HCl | 0.1 (M) |