1OY1
X-Ray Structure Of ElbB From E. Coli. Northeast Structural Genomics Research Consortium (Nesg) Target Er105
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 2002-11-22 |
| Detector | BRANDEIS - B4 |
| Wavelength(s) | 0.97900, 0.78911, 0.9200 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 99.108, 105.522, 165.102 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.950 |
| Rwork | 0.216 |
| R-free | 0.26500 |
| Structure solution method | MAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.366 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 3.010 |
| High resolution limit [Å] | 2.950 | 2.950 |
| Number of reflections | 18121 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP, 3.3 M SODIUM FORMATE, 12mM pyridoxal at 30C |
