1OXA

CYTOCHROME P450 (DONOR:O2 OXIDOREDUCTASE)

Experimental procedure

Detector technology	AREA DETECTOR
Detector	SIEMENS-NICOLET X100
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	54.160, 79.670, 99.480
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.100
R-factor	0.196
Rwork	0.196
RMSD bond length	0.007
RMSD bond angle	1.342
Data reduction software	XENGEN
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.100
Rmerge	0.054
Total number of observations	127949 *
Number of reflections	23771
Completeness [%]	91.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	24 (%)
2	1	reservoir	sodium acetate	0.2 (M)
3	1	reservoir	Tris-HCl	0.1 (M)