1ONR

STRUCTURE OF TRANSALDOLASE B

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1995-01-12
Detector	RIGAKU RAXIS II
Spacegroup name	P 21 21 21
Unit cell lengths	68.900, 91.300, 130.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	5.500 - 1.870
R-factor	0.201
Rwork	0.201
R-free	0.23400
RMSD bond length	0.006
RMSD bond angle	1.506
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.870 *	1.870 *
Rmerge	0.064
Total number of observations	498214 *
Number of reflections	62509
Completeness [%]	91.3	82.8 *
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	4 *	293 *	Jia, J., (1996) Acta Crystallogr.,Sect.D, 52, 192. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium citrate	0.1 (M)
2	1	reservoir	PEG6000	15 (%)
3	1	drop	enzyme	20 (mg/ml)