1OFS
Pea lectin-sucrose complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2002-07-15 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.831, 60.803, 136.087 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.860 - 1.800 |
R-factor | 0.168 |
Rwork | 0.166 |
R-free | 0.20657 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1LTN |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 1.830 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.480 | 0.207 |
Number of reflections | 38608 | |
<I/σ(I)> | 22.8 | 5.53 |
Completeness [%] | 98.1 | 89.4 |
Redundancy | 3.57 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.1 M MES PH 6.5, 12% (W/V) PEG 20K, 8% (V/V) ETOH, 40 MM SUCROSE; CRYOSOLUTION: 0.1 M MES PH 6.5, 17% PEG 20K, 60% (V/V) ETOH, 25 MM SUCROSE |