Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X13 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X13 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-01-01 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 85.334, 93.070, 98.795 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.400 |
| R-factor | 0.156 |
| Rwork | 0.156 |
| R-free | 0.16100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6xia |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.770 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.430 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Rmerge | 0.050 | |
| Number of reflections | 154724 | |
| <I/σ(I)> | 43.8 | 12.7 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 14.5 | 14.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7 | MPD, MgCl2, TRIS, pH 7.00 |
