1NQ7
Characterization of ligands for the orphan nuclear receptor RORbeta
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2002-12-18 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.0100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 52.823, 58.343, 105.668 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 * - 1.500 |
| R-factor | 0.201 |
| Rwork | 0.201 |
| R-free | 0.22000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1k4w |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.077 * |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.550 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.061 * | 0.167 * |
| Number of reflections | 53123 * | |
| <I/σ(I)> | 32 | |
| Completeness [%] | 100.0 * | 100 |
| Redundancy | 8.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 8 | 293 | Potier, N., (2003) Protein Sci., 12, 725. * |
