1NCH
STRUCTURAL BASIS OF CELL-CELL ADHESION BY CADHERINS
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Detector technology | IMAGE PLATE |
| Collection date | 1994-08 |
| Detector | FUJI |
| Wavelength(s) | 0.98 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 79.730, 79.730, 74.960 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 5.000 - 2.100 |
| R-factor | 0.224 |
| Rwork | 0.224 |
| R-free | 0.30900 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 2.130 |
| Data reduction software | DENZO |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Rmerge | 0.047 |
| Number of reflections | 15198 |
| Completeness [%] | 93.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 20 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein solution | 0.002-0.003ml | |
| 2 | 1 | reservoir | 0.8 (M) | ||
| 3 | 1 | reservoir | sodium acetate | 0.1 (M) | |
| 4 | 1 | reservoir | Yb acetate | 20 (mM) |
