1MU6
Crystal Structure of Thrombin in Complex with L-378,622
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 290 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999 |
| Detector | RIGAKU RAXIS II |
| Wavelength(s) | 1.542 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.220, 72.210, 73.300 |
| Unit cell angles | 90.00, 101.10, 90.00 |
Refinement procedure
| Resolution | 29.290 - 1.990 |
| R-factor | 0.206 |
| Rwork | 0.206 |
| R-free | 0.23500 |
| Structure solution method | FOURIER SYNTHESIS |
| Refinement software | CNX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.290 |
| High resolution limit [Å] | 1.990 |
| Number of reflections | 22747 |
| Completeness [%] | 91.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 295 | pH 7.3, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
