1MKB

ESCHERICHIA COLI BETA-HYDROXYDECANOYL THIOL ESTER DEHYDRASE AT PH 5 AND 21 DEGREES C

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1994-09
Detector	RIGAKU RAXIS
Spacegroup name	P 21 21 21
Unit cell lengths	68.500, 86.900, 60.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 - 2.000
R-factor	0.183
Rwork	0.183
R-free	0.24300
RMSD bond length	0.010
RMSD bond angle	1.630
Data reduction software	DENZO
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.000 *
Rmerge	0.063
Number of reflections	23461 *
Completeness [%]	93.0 *
Redundancy	2.7 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	2.5 (mg/ml)
2	1	1	3-decynoylNAC	3.7 (mM)
3	1	1	aceton	2 (%(v/v))