1LPM

A STRUCTURAL BASIS FOR THE CHIRAL PREFERENCES OF LIPASES

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	65.200, 97.500, 176.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.200 *
R-factor	0.139
Rwork	0.139
RMSD bond length	0.011
RMSD bond angle	1.820
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	8.000 *
High resolution limit [Å]	2.200 *
Rmerge	0.107 *
Total number of observations	68189 *
Number of reflections	25316
Completeness [%]	84.8
Redundancy	2.7 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	5.3 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	8 (mg/ml)
2	1	reservoir	MPD	40 (%(v/v))
3	1	reservoir	sodium acetate	30 (mM)
4	1	reservoir		30 (mM)