1LIO

STRUCTURE OF APO T. GONDII ADENOSINE KINASE

Replaces:  1DH2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Temperature [K]	298
Detector technology	IMAGE PLATE
Collection date	1998-11-10
Detector	RIGAKU RAXIS IV
Spacegroup name	P 1 21 1
Unit cell lengths	47.100, 68.000, 56.800
Unit cell angles	90.00, 100.80, 90.00

Refinement procedure

Resolution	10.000 - 2.500
R-factor	0.2
Rwork	0.198
R-free	0.26000
RMSD bond length	0.011
RMSD bond angle	1.903
Data reduction software	bioteX
Data scaling software	bioteX
Phasing software	MERLOT
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000	2.700
High resolution limit [Å]	2.500	2.500
Rmerge	0.099	0.230
Number of reflections	28789
<I/σ(I)>	10
Completeness [%]	95.0	85
Redundancy	2	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.50