1LGC

INTERACTION OF A LEGUME LECTIN WITH THE N2 FRAGMENT OF HUMAN LACTOTRANSFERRIN OR WITH THE ISOLATED BIANTENNARY GLYCOPEPTIDE: ROLE OF THE FUCOSE MOIETY

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	117.000, 117.000, 120.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.800
R-factor	0.185
Rwork	0.185
RMSD bond length	0.009
RMSD bond angle	1.900
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000 *
High resolution limit [Å]	2.800 *
Rmerge	0.130 *
Total number of observations	132152 *
Number of reflections	24967 *
Completeness [%]	98.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	6.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	MPD	30-35 (%(v/v))
2	1	drop	protein	20 (mg/ml)