1KSN

Crystal Structure of Human Coagulation Factor XA Complexed with FXV673

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1999-07-01
Detector	MACSCIENCE DIP100S
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	55.810, 71.600, 79.030
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.000 - 2.100
R-factor	0.223
Rwork	0.223
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	X-PLOR (98)

Data quality characteristics

	Overall
Low resolution limit [Å]	28.000
High resolution limit [Å]	2.100
Number of reflections	15384
Completeness [%]	81.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.7	292	18-20% PEG 600, 50MM MES-NAOH, 1MM RPR128515, pH 5.7, VAPOR DIFFUSION, HANGING DROP, temperature 292K