1KPT
STRUCTURE AND FUNCTION OF A VIRALLY ENCODED FUNGAL TOXIN FROM USTILAGO MAYDIS: A FUNGAL AND MAMMALIAN CALCIUM CHANNEL INHIBITOR
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-02-21 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 26.140, 63.760, 53.620 |
Unit cell angles | 90.00, 92.20, 90.00 |
Refinement procedure
Resolution | 6.000 - 1.900 * |
R-factor | 0.186 * |
Rwork | 0.174 |
R-free | 0.23700 * |
RMSD bond length | 0.019 * |
RMSD bond angle | 1.950 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 1.700 |
Rmerge | 0.052 |
Number of reflections | 15905 |
Completeness [%] | 81.9 * |
Redundancy | 3.42 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium citrate | 0.2 (M) | |
2 | 1 | reservoir | isopropanol | 20 (%) | |
3 | 1 | reservoir | HEPES | 0.1 (M) | |
4 | 1 | drop | KP4 toxin | 10 (mg/ml) | |
5 | 1 | drop | sodium citrate | 0.2 (M) | |
6 | 1 | drop | isopropanol | 20 (%) | |
7 | 1 | drop | HEPES | 0.1 (M) |