1JSZ
Crystal Structure Analysis of N7,9-dimethylguanine-VP39 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 113 |
Detector technology | CCD |
Collection date | 1999-01-01 |
Detector | SIEMENS |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 84.300, 67.700, 79.600 |
Unit cell angles | 90.00, 118.10, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.930 |
R-factor | 0.214 |
Rwork | 0.210 |
R-free | 0.25200 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 24.380 * |
Data reduction software | SAINT ((SIEMENS)) |
Data scaling software | SAINT ((SIEMENS)) |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.990 |
High resolution limit [Å] | 1.930 | 1.930 |
Rmerge | 0.081 * | |
Number of reflections | 22339 | |
Completeness [%] | 73.5 | 50 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.5 | 298 | Hodel, A.E., (1996) Cell(Cambridge,Mass.), 85, 247. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG8000 | 10 (%) | |
2 | 1 | 1 | 0.125 (M) | ||
3 | 1 | 1 | citrate | 0.1 (M) |