1JOB

Crystal Structure of Murine Olfactory Marker Protein in Spacegroup P3121

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X12B
Synchrotron site	NSLS
Beamline	X12B
Temperature [K]	130
Detector technology	CCD
Collection date	2000-03-29
Detector	ADSC QUANTUM 4
Wavelength(s)	1.276
Spacegroup name	P 31 2 1
Unit cell lengths	86.327, 86.327, 71.574
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.000 - 2.400
R-factor	0.234
Rwork	0.234
R-free	0.26400
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1f35
RMSD bond length	0.017
RMSD bond angle	1.700
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	X-PLOR (3.851)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.490
High resolution limit [Å]	2.400	2.400
Number of reflections	11701
<I/σ(I)>	12.6
Completeness [%]	94.4
Redundancy	19.31

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5	295	unpublished structure *