1JDO
SPERM WHALE MYOGLOBIN (FERROUS, NITRIC OXIDE BOUND)
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 295 |
| Detector technology | IMAGE PLATE |
| Collection date | 1997-02-14 |
| Detector | RIGAKU |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.506, 91.506, 45.853 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 5.000 - 1.900 |
| R-factor | 0.1531 |
| R-free | 0.20590 |
| Structure solution method | DIFFERENCE FOURIER |
| Starting model (for MR) | 2spl |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.018 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXL-96 |
| Refinement software | SHELXL-96 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.064 | 0.292 |
| Number of reflections | 17289 | |
| <I/σ(I)> | 26.4 | 5.5 |
| Completeness [%] | 99.0 | 99.8 |
| Redundancy | 4.2 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 9 | pH 9. |
