1ITH
STRUCTURE DETERMINATION AND REFINEMENT OF HOMOTETRAMERIC HEMOGLOBIN FROM URECHIS CAUPO AT 2.5 ANGSTROMS RESOLUTION
Experimental procedure
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 104.800, 54.900, 110.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 5.000 * - 2.500 |
| R-factor | 0.147 |
| Rwork | 0.147 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 3.330 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.8 * | taken from Kolatkar, P.P. et al(1988), J. Biol. Chem., 263, 3462-3465. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | 10 (mM) | ||
| 2 | 1 | 1 | Tris-HCl | 10 (mM) | |
| 3 | 1 | 1 | PEG8000 | 10 (%) |
