1HBV
A CHECK ON RATIONAL DRUG DESIGN. CRYSTAL STRUCTURE OF A COMPLEX OF HIV-1 PROTEASE WITH A NOVEL GAMMA-TURN MIMETIC
Experimental procedure
| Detector technology | AREA DETECTOR |
| Collection date | 1993-12-08 |
| Detector | SIEMENS |
| Spacegroup name | P 61 |
| Unit cell lengths | 63.400, 63.400, 83.900 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.300 |
| R-factor | 0.177 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 3.550 |
| Data reduction software | XENGEN |
| Phasing software | X-PLOR |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 9999.000 * |
| High resolution limit [Å] | 2.300 * |
| Rmerge | 0.095 |
| Total number of observations | 36970 * |
| Number of reflections | 8051 |
| Completeness [%] | 94.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 16-28 (%) | precipitant |
| 2 | 1 | reservoir | sodium acetate | 200 (mM) | precipitant |
