1H9H
COMPLEX OF EETI-II WITH PORCINE TRYPSIN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-2 |
| Synchrotron site | ESRF |
| Beamline | ID14-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1999-04-04 |
| Detector | MARRESEARCH |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 121.050, 121.050, 121.050 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.500 |
| R-factor | 0.2331 |
| R-free | 0.27580 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1ldt |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.028 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.600 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.053 | 0.376 |
| Number of reflections | 49533 | |
| <I/σ(I)> | 19.24 | 3.39 |
| Completeness [%] | 99.7 | 99.6 |
| Redundancy | 8.05 | 4.48 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.7 | pH 6.70 |
