1H8T

Echovirus 11

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID2
Synchrotron site	ESRF
Beamline	ID2
Temperature [K]	287
Detector technology	IMAGE PLATE
Collection date	1997-10-15
Detector	MARRESEARCH
Spacegroup name	H 3 2
Unit cell lengths	300.850, 300.850, 1476.620
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	500.000 * - 2.900
R-factor	0.2462
Rwork	0.246
R-free	0.25490
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1d4m
RMSD bond length	0.017 *
RMSD bond angle	2.000 *
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	X-PLOR
Refinement software	CNS (1.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	3.200
High resolution limit [Å]	2.900	2.900
Rmerge	0.220	0.350
Total number of observations	1648270 *
Number of reflections	411040
Completeness [%]	70.0	35
Redundancy	4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	7.4 *		2.0M AMMONIUM SULPHATE, pH 7.50

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Tris-Cl	10 (mM)	pH7.4
2	1	reservoir	ammonium sulfate	2.0 (M)