1GWF
Compound II structure of Micrococcus Lysodeikticus catalase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 1995-10-15 |
Detector | MARRESEARCH |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 106.190, 106.190, 105.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.540 - 1.960 |
R-factor | 0.08935 |
Rwork | 0.141 |
R-free | 0.18966 |
Structure solution method | OTHER |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 74.536 |
High resolution limit [Å] | 1.936 |
Rmerge | 0.061 |
Number of reflections | 41376 |
<I/σ(I)> | 8 |
Completeness [%] | 99.5 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.2 | pH 5.20 |