1GMU
Structure of UreE
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | MPG/DESY, HAMBURG BEAMLINE BW6 |
| Synchrotron site | MPG/DESY, HAMBURG |
| Beamline | BW6 |
| Temperature [K] | 100 |
| Wavelength(s) | 1.0500, 0.9500, 0.9815, 0.9805 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.882, 129.360, 56.786 |
| Unit cell angles | 90.00, 93.72, 90.00 |
Refinement procedure
| Resolution | 17.000 - 1.500 |
| R-factor | 0.223 |
| Rwork | 0.223 |
| R-free | 0.26100 |
| Structure solution method | MAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.302 |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 17.000 |
| High resolution limit [Å] | 1.500 |
| Rmerge | 0.026 |
| Number of reflections | 97562 |
| Completeness [%] | 96.9 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | pH 6.50 |
