1GIC
CONCANAVALIN A COMPLEXED WITH METHYL ALPHA-D-GLUCOPYRANOSIDE
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.6 |
| Synchrotron site | SRS |
| Beamline | PX9.6 |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1988 |
| Detector | SIEMENS |
| Spacegroup name | I 21 3 |
| Unit cell lengths | 167.800, 167.800, 167.800 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 100.000 - 2.000 |
| R-factor | 0.17 |
| Rwork | 0.170 |
| Structure solution method | MIR + MR |
| Starting model (for MR) | 1con |
| RMSD bond length | 0.014 |
| RMSD bond angle | 3.200 |
| Data reduction software | XENGEN ((TO 5.2A)) |
| Data scaling software | CCP4 ((AGROVATA) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Rmerge | 0.046 |
| Number of reflections | 34648 |
| Completeness [%] | 64.0 |
| Redundancy | 30 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | dialysis | 6.8 | DIALYSIS; 5MM PROTEIN CONCENTRATION WITH, pH 6.8, dialysis |
