1FXR

CRYSTAL STRUCTURE OF THE FERREDOXIN I FROM DESULFOVIBRIO AFRICANUS AT 2.3 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	96.600, 58.100, 20.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.300
R-factor	0.182
Rwork	0.182
R-free	0.22700
RMSD bond length	0.013
RMSD bond angle	2.930
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.086 *
Completeness [%]	70.6 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	26.6 (mg/ml)
2	1	reservoir	ammonium sulfate	53-65 (%sat)
3	1	reservoir	sodium acetate	0.1 (M)