1FUG
S-ADENOSYLMETHIONINE SYNTHETASE
Experimental procedure
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1994-10 |
Detector | MACSCIENCE DIP100 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 121.000, 121.000, 171.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 3.200 |
R-factor | 0.21 |
Rwork | 0.210 |
R-free | 0.29000 |
RMSD bond length | 0.015 |
RMSD bond angle | 25.000 * |
Data reduction software | ELMS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 8.000 | 3.300 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.080 | 0.110 |
Total number of observations | 52893 * | |
Number of reflections | 18581 | |
<I/σ(I)> | 2.7 | |
Completeness [%] | 92.4 | 85 |
Redundancy | 3 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7 | 4 * | pH 7.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | potassium phosphate | 100 (mM) | |
2 | 1 | 1 | 10 (mM) | ||
3 | 1 | 1 | ammonium sulfate | 33 (%(v/v)sat) | |
4 | 1 | 2 | protein | 10 (mg/ml) |