1FLL

MOLECULAR BASIS FOR CD40 SIGNALING MEDIATED BY TRAF3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	108
Detector technology	IMAGE PLATE
Collection date	1999-05-27
Detector	MARRESEARCH
Spacegroup name	P 3 2 1
Unit cell lengths	83.760, 83.760, 212.570
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 3.500
R-factor	0.173
Rwork	0.173
R-free	0.31200
RMSD bond length	0.008
RMSD bond angle	1.550
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.630
High resolution limit [Å]	3.500	3.500
Rmerge	0.078	0.260
Number of reflections	29115
<I/σ(I)>	14
Completeness [%]	78.7	74.5
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.5	294	METHANOL, SODIUM CHLORIDE, TRIS BUFFER, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K