1FLK
MOLECULAR BASIS FOR CD40 SIGNALING MEDIATED BY TRAF3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-1 |
| Synchrotron site | SSRL |
| Beamline | BL9-1 |
| Temperature [K] | 108 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-05-20 |
| Detector | MARRESEARCH |
| Spacegroup name | H 3 |
| Unit cell lengths | 84.530, 84.530, 319.500 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.800 |
| R-factor | 0.224 |
| Rwork | 0.224 |
| R-free | 0.28600 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.400 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.890 |
| High resolution limit [Å] | 2.800 | 2.790 |
| Rmerge | 0.051 | 0.240 |
| Number of reflections | 58040 | |
| <I/σ(I)> | 18.9 | |
| Completeness [%] | 98.3 | 89.1 |
| Redundancy | 2.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.5 | 294 | METHANOL, SODIUM CHLORIDE, TRIS BUFFER, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K |
