1FKJ
ATOMIC STRUCTURE OF FKBP12-FK506, AN IMMUNOPHILIN IMMUNOSUPPRESSANT COMPLEX
Experimental procedure
| Detector technology | IMAGE PLATE |
| Spacegroup name | P 42 21 2 |
| Unit cell lengths | 58.100, 58.100, 55.700 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 7.000 - 1.700 |
| R-factor | 0.162 |
| Rwork | 0.162 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.150 * |
| Data reduction software | MANUFACTURER (SUPPLIED (MSC)) |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 20 (mg/ml) | |
| 2 | 1 | reservoir | ammonium sulfate | 1.7 (M) | |
| 3 | 1 | reservoir | cacodylate | 200 (mM) |
