1FK5
STRUCTURAL BASIS OF NON-SPECIFIC LIPID BINDING IN MAIZE LIPID-TRANSFER PROTEIN COMPLEXES WITH OLEIC ACID REVEALED BY HIGH-RESOLUTION X-RAY CRYSTALLOGRAPHY
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1999-12-02 |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.676, 49.717, 69.204 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.300 |
R-factor | 0.135 |
Rwork | 0.135 |
R-free | 0.18800 |
Structure solution method | MR |
Starting model (for MR) | (PDB CODE:1MZL) |
RMSD bond length | 0.009 |
RMSD bond angle | 2.200 |
Data reduction software | WEIS |
Data scaling software | WEIS |
Phasing software | X-PLOR |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.300 |
Rmerge | 0.057 |
Total number of observations | 93324 * |
Number of reflections | 18062 |
Completeness [%] | 75.7 |
Redundancy | 5.17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 24.5-25.5 * | 3.6-4.8M Na formate, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | sodium formate | 3.6-4.8 (M) |