1FEM

CRYSTALLOGRAPHIC STUDIES ON COMPLEXES BETWEEN RETINOIDS AND PLASMA RETINOL-BINDING PROTEIN

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	46.210, 48.810, 75.810
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	9.000 - 1.900
R-factor	0.184
RMSD bond length	0.008 *
RMSD bond angle	2.800 *
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.900 *
Rmerge	0.105 *
Total number of observations	16527 *
Number of reflections	7294 *
Completeness [%]	43.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	bRBP	6-10 (mg/ml)
2	1	2	sodium chloride	0.1 (M)
3	1	2	cadmium acetate	0.01-1. (mM)
4	1	2	sodium acetate	0.1 (M)