1FBP
CRYSTAL STRUCTURE OF FRUCTOSE-1,6-BISPHOSPHATASE COMPLEXED WITH FRUCTOSE 6-PHOSPHATE, AMP, AND MAGNESIUM
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 61.600, 166.600, 80.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 * - 2.500 |
R-factor | 0.215 * |
Rwork | 0.215 |
RMSD bond length | 0.013 |
RMSD bond angle | 3.500 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.061 * |
Total number of observations | 87690 * |
Number of reflections | 27511 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 7.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | AMP | 1 (mM) | |
2 | 1 | 1 | F6P | 1 (mM) | |
3 | 1 | 1 | 5 (mM) | ||
4 | 1 | 1 | Fru-1,6-Pase | ||
5 | 1 | 2 | Tris | 20 (mM) | |
6 | 1 | 2 | maleic acid | 2 (mM) | |
7 | 1 | 2 | EDTA | 0.1 (mM) | |
8 | 1 | 2 | 5 (mM) | ||
9 | 1 | 2 | PEG3350 | 9.5 (%(w/v)) |