1EX0
HUMAN FACTOR XIII, MUTANT W279F ZYMOGEN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-1 |
Synchrotron site | SSRL |
Beamline | BL9-1 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-04-17 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 100.540, 70.640, 133.380 |
Unit cell angles | 90.00, 106.08, 90.00 |
Refinement procedure
Resolution | 19.940 - 2.000 |
Rwork | 0.187 |
R-free | 0.23400 |
RMSD bond length | 0.013 |
RMSD bond angle | 2.500 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (V 3.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.510 | 1.840 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.048 | 0.402 |
Number of reflections | 158697 | |
<I/σ(I)> | 11.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 295 | 10 - 12 % 1,2-propanediol, 0.1 M Na-K phosphate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K |