1EPO
ENDOTHIA ASPARTIC PROTEINASE (ENDOTHIAPEPSIN) COMPLEXED WITH CP-81,282 (MOR PHE NLE CHF NME)
Experimental procedure
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.700, 73.900, 45.800 |
Unit cell angles | 90.00, 110.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.18 |
RMSD bond length | 0.021 |
RMSD bond angle | 0.023 |
Refinement software | RESTRAIN |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.000 * |
Rmerge | 0.074 * |
Total number of observations | 42676 * |
Number of reflections | 16999 * |
Completeness [%] | 76.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.3 * | pH is adjusted to 6.3 with dilute sodium hydroxide * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | ammonium sulfate | 2.2 (M) | |
2 | 1 | 1 | acetate | or phosphate | |
3 | 1 | 1 | sodium dihydrogen phosphate | 0.1 (M) | |
4 | 1 | 1 | acetone | 0.25-0.1 (%(w/v)) |