1ECM
ATOMIC STRUCTURE OF THE BURIED CATALYTIC POCKET OF ESCHERICHIA COLI CHORISMATE MUTASE
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-02-01 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 80.830, 80.830, 83.320 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
R-factor | 0.192 |
Rwork | 0.192 |
R-free | 0.23100 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.600 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Rmerge | 0.050 |
Number of reflections | 23622 |
Completeness [%] | 98.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.85 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein-inhibitor solution | 10.5 (mg/ml) | |
2 | 1 | reservoir | sodium cacodylate | 100 (mM) | |
3 | 1 | reservoir | sodium acetate | 200 (mM) | |
4 | 1 | reservoir | PEG8000 | 28-30 (%) |