1EB3
YEAST 5-AMINOLAEVULINIC ACID DEHYDRATASE 4,7-DIOXOSEBACIC ACID COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-04-29 |
Detector | ADSC CCD |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 104.300, 104.300, 167.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.300 - 1.750 |
R-factor | 0.239 |
R-free | 0.30800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ylv |
RMSD bond length | 0.008 |
RMSD bond angle | 0.021 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CCP4 |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.400 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.114 | 0.364 |
Number of reflections | 44379 | |
<I/σ(I)> | 4.6 | 1.6 |
Completeness [%] | 95.5 | 98.5 |
Redundancy | 6.2 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | AS FOR PDB ENTRY 1AW5 WITH 5 MM 4,7-DIOXO-SEBACIC ACID IN DROP, pH 8.00 |