1DZL
L1 protein of human papillomavirus 16
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE F2 |
| Synchrotron site | CHESS |
| Beamline | F2 |
| Temperature [K] | 100 |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 387.000, 387.000, 387.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 15.000 - 3.500 |
| R-factor | 0.283 * |
| Rwork | 0.280 |
| R-free | 0.29100 * |
| Structure solution method | SIR |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.200 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 70.000 | |
| High resolution limit [Å] | 3.500 | 3.500 * |
| Rmerge | 0.120 * | 0.410 * |
| Number of reflections | 202000 | |
| Completeness [%] | 87.5 * | 56 * |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 4.5 | pH 4.50 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PEG | 7.5 (%) | |
| 2 | 1 | 1 | 0.2 (M) |
