1DTJ
CRYSTAL STRUCTURE OF NOVA-2 KH3 K-HOMOLOGY RNA-BINDING DOMAIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F2 |
Synchrotron site | CHESS |
Beamline | F2 |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 1998-04-01 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 66.500, 61.100, 97.300 |
Unit cell angles | 90.00, 98.20, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.000 |
R-factor | 0.229 |
Rwork | 0.225 |
R-free | 0.27900 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.800 |
Data reduction software | DENZO |
Data scaling software | CCP4 ((TRUNCATE)) |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.088 | 0.197 |
Number of reflections | 25590 | |
<I/σ(I)> | 15.4 | |
Completeness [%] | 99.0 | 99.2 |
Redundancy | 4.1 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 3 | 4 * | (NH4)2SO4, MPD, sodium chloride, pH 3.0, VAPOR DIFFUSION, temperature 277.0K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 1.4 (M) | |
2 | 1 | reservoir | MPD | 2 (%) | |
3 | 1 | reservoir | Formic acid | 50 (mM) |