1D2Q
CRYSTAL STRUCTURE OF HUMAN TRAIL
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | MACSCIENCE |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | MACSCIENCE |
| Spacegroup name | P 63 |
| Unit cell lengths | 65.610, 65.610, 131.700 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | ? - 2.800 |
| Rwork | 0.209 |
| R-free | 0.28200 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.662 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmerge | 0.063 | |
| Completeness [%] | 89.6 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 9 | 295 | PEG 550 MME, bicine pH 9.0, cadmium chloride, EVAPORATION, temperature 22K |
| 1 | unknown * | 9 | 295 | PEG 550 MME, bicine pH 9.0, cadmium chloride, EVAPORATION, temperature 22K |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | mPEG550 | 25 (%) | |
| 2 | 1 | 1 | bicine | 0.05 (M) | |
| 3 | 1 | 1 | 10 (mM) |
