1D14
STRUCTURE OF 11-DEOXYDAUNOMYCIN BOUND TO DNA CONTAINING A PHOSPHOROTHIOATE
Experimental procedure
Temperature [K] | 283 |
Detector technology | DIFFRACTOMETER |
Detector | NICOLET P3 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 17.730, 19.130, 26.360 |
Unit cell angles | 90.00, 98.01, 90.00 |
Refinement procedure
Resolution | 1.700 * - 1.500 |
R-factor | 0.224 |
RMSD bond length | 0.038 * |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.500 |
Number of reflections | 2129 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6 | pH 6.00, VAPOR DIFFUSION |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | SPERMINE | ||
5 | 1 | 1 | MGCL2 | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | 1.5 (mM) | single strand |
2 | 1 | drop | sodium cacodylate | 20 (mM) | |
3 | 1 | drop | 6.0 (mM) | ||
4 | 1 | drop | spermine | 1.5 (mM) | |
5 | 1 | drop | MPD | 20 (%) | |
6 | 1 | reservoir | MPD | 30 (%) |