1D11
INTERACTIONS BETWEEN AN ANTHRACYCLINE ANTIBIOTIC AND DNA MOLECULAR STRUCTURE OF DAUNOMYCIN COMPLEXED TO D(CPGPTPAPCPG) AT 1.2-ANGSTROMS RESOLUTION
Experimental procedure
Temperature [K] | 288 |
Detector technology | DIFFRACTOMETER |
Detector | NICOLET P3X |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 27.860, 27.860, 52.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.200 * |
R-factor | 0.175 |
RMSD bond length | 0.034 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.200 |
Number of reflections | 9238 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | other * | 6.5 | pH 6.50, VAPOR DIFFUSION |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MGCL2 | ||
4 | 1 | 1 | SPERMINE | ||
5 | 1 | 1 | NA CACODYLATE | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | DNA hexamer | (mM) | single strand | |
2 | 1 | daunomycin | 2 (mM) | ||
4 | 1 | spermine | 10 (mM) | ||
5 | 1 | cacodylate | 30 (mM) | ||
6 | 1 | 1 | MPD | 5 (%) |