1CT2
CRYSTAL STRUCTURE OF THE OMTKY3 P1 VARIANT OMTKY3-THR18I IN COMPLEX WITH SGPB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1997-06-24 |
Detector | MAC Science DIP-2000H |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 45.656, 54.530, 45.589 |
Unit cell angles | 90.00, 119.24, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.650 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.954 |
Data reduction software | DIP (XPRESS) |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.068 | 0.326 |
Total number of observations | 68327 * | |
Number of reflections | 21917 * | |
<I/σ(I)> | 13.24 | |
Completeness [%] | 91.5 | 59.9 |
Redundancy | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 298 | PEG 4000 sodium potassium phosphate , pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 9 (mg/ml) | |
2 | 1 | reservoir | PEG4000 | 4-10 (%) |